The IV Line News from the Lab
Inorganic Ventures' E-newsletter  •  Winter 2005  •  inorganicventures.com
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In this issue...
 News from the Lab  Articles Online
 Analytical Quick Tip  IV Line Humor
 Is your standard as good as you think?

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News from the Lab

Standards Across the Globe

PittCon 2005
Free Giveaways at Booth 4177
We're gearing up to appear at PittCon 2005. Visit us at booth 4177 and find out how you can receive a FREE 125mL standard. We'd love to see you in person.

The Pittsburgh Conference will be held at the Orange County Convention Center in Orlando, Florida from February 27 through March 4, 2005. details »

Analytical Quick Tip

Segregate glassware used for trace metals analysis. Glassware can be a major source of contamination. In addition, it is suggested that glassware used with HCl be segregated from that used with nitric acid, sulfuric acid, etc. This will help avoid potential losses of Ag as the chloride and Pb as the sulfate.

Is your standard as good as you think?

Concerned with the accuracy of your analyses? Remember, the quality of your standard will directly affect your results. But how can you gauge a standard's quality before you use it?

The International Standard Organization (ISO) provides worldwide guidelines for quality. Manufacturers can choose to apply for accreditations that are specific to their industry. After passing a series of rigorous audits, they'll receive the appropriate ISO accreditation. These accreditations help prove the validity of their "quality" claims to you, the consumer. But which ISO credentials are important?

Ideally, manufacturers of chemical standards (also known as certified reference materials or CRMs) should be accredited to three:
Three levels of ISO

  1. GOOD:  ISO 9001:2000

    Certifies that a manufacturer is running a business with quality-conscious procedures in place. However, this accreditation says nothing about laboratory proficiency or CRM production.

  2. BETTER:  ISO 17025:1999

    To be ISO 17025 certified, a manufacturer must be proficient in laboratory testing as well as testing the quality of their products. Still, this guide does not require competency specific to CRM manufacturing.

  3. BEST:  ISO Guide 34:2000

    This is the only accreditation that deals directly with the production of CRMs. All methods that the manufacturer uses to certify their standards must be validated and proven to be accurate. Surprisingly, very few CRM producers carry this key accreditation.

So the next time you're facing a decisive analysis, consider using a standard made by an ISO-accredited manufacturer. The more accreditations they hold, the more confident you can be in their product.

Inorganic Ventures is one of the only standard manufacturers to carry all three of these ISO accreditations.

Articles Online  more articles »

Traceability
Part sixteen, the final installment of our ICP Operations guide, outlines the concept of traceability as it relates to certified reference materials.

Reactions of Sulfur and Bromine
Dr. Gaines offers his expertise regarding sulfur-containing compounds, specifically concerning the reaction between sulfur and bromine.

Analysis of Sediment Samples
Dr. Gaines provides some recommendations when analyzing sediment samples for cesium.

IV Line Humor  more humor »

Florence Flask was getting ready for the opera. All of a sudden, she screamed: "Erlenmeyer, my joules! Somebody has stolen my joules!" The husband replied, "Calm down, honey. We'll find a solution."

Elemental Spotlight
Praeseo-dymium

Analytical Periodic Table

Storage & Handling:  Keep tightly sealed when not in use. Store and use at 20 ± 4°C. Do not pipet from container. Do not return portions removed for pipetting to container.

Chemical Compatibility:  Soluble in HCl and HNO3. Avoid HF, H3PO4, H2SO4, and neutral to basic media. Stable with most metals and inorganic anions forming an insoluble carbonate, oxide, oxalate, and fluoride and sparingly soluble sulfates (La - Eu exhibit low sulfate solubility). Avoid mixing with elements / solutions containing moderate amounts of fluoride.

Stability:  2-100 ppb levels stable for months in 1% HNO3 / LDPE container. 1-10,000 ppm solutions chemically stable for years in 2-5% HNO3 / LDPE container.

Pr Containing Samples (Preparation & Solution):  Metal (soluble in acids); Oxide (dissolved by heating in H2O / HNO3); Ores (carbonate fusion in Pt0 followed by HCl dissolution); Organic Matrices (dry ash and dissolve in 1:1 H2O / HCl or HNO3).

Excerpt from Inorganic Venture's Analytical Periodic Table: Includes detailed analytical data for more than 70 elements.
 
Elemental Wordplay
Rearrange the elemental symbols to solve the riddle. Clues appear in quotes.

If you're "riding" in this, you're likely enjoying the "comforts" of a...

    - Molybdenum
    - Neon
    - Silicon
    - Uranium
    - and Lithium.

(answer at bottom of page)
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 Wordplay answer:  Postage (Li,Mo,U,Si,Ne)
 The IV Line · News from the Lab  · Winter 2005 (volume 12)
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Inorganic Ventures
195 Lehigh Ave · Suite 4
Lakewood, NJ 08701

   1.800.669.6799 
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